DWSIM/C2/Shortcut-Distillation/English-timed

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Time Narration
00:01 Welcome to this tutorial on Simulating a Shortcut Distillation column in DWSIM.
00:07 In this tutorial, we will learn to:
00:10 Simulate a Shortcut distillation column
00:13 Calculate Minimum number of stages
00:16 Calculate Minimum reflux ratio
00:19 Calculate Optimal Feed stage location
00:22 Calculate Condenser and Reboiler duty
00:26 This tutorial is recorded using

DWSIM version 5. 8 (Classic UI) Update 3 and Windows 10 OS

00:37 But, this process is identical in Linux, Mac OS X or FOSSEE OS on ARM.
00:43 To practise this tutorial, you should know to-
00:47 Add components to a flowsheet
00:50 Select thermodynamic packages
00:53 Add material and energy streams and specify their properties.
00:58 The prerequisite DWSIM tutorials are available on this website.
01:03 You can access these tutorials and all the associated files from this site.
01:09 We will develop a flowsheet to determine Outlet stream properties after Shortcut Distillation.
01:15 Here we give Compounds, Thermodynamics and Inlet stream conditions.
01:21 Next, we give Shortcut Column Properties.
01:25 I have already opened DWSIM.
01:28 Go to File menu and select New Steady-state Simulation.
01:33 Simulation Configuration Wizard window opens.
01:35 Click on Next button at the bottom.
01:40 In the Compounds Search tab, type Benzene.
01:45 Select Benzene from ChemSep database.
01:49 Similarly, add Toluene.
01:52 Click the Next button at the bottom.
01:56 Now comes Property Packages.
01:59 From Available Property Packages list, double-click on Raoult’s Law.
02:04 At the bottom, click on the Next button.
02:08 Next option is System of Units.
02:12 Under System of Units, select C5.
02:17 Pressure menu appears at the top of this list.
02:20 Select atm for atmosphere and press Enter.
02:25 Lastly, at the bottom, click on the Finish button.
02:30 Now maximize the Simulation window.
02:33 Now let’s insert a feed stream that has to be distilled.
02:38 At the bottom of the main simulation window, go to Streams.
02:43 From the displayed list, drag and drop a Material Stream to the Flowsheet.
02:48 Click on the material stream named MSTR 000.
02:53 Let’s change the name of this stream to Feed.

Press Enter.

02:59 Now we will specify the Feed stream compositions.
03:03 For this under Input Data click on Compound Amounts tab.
03:09 Choose the Basis as Mole Fractions, if not already selected.
03:14 By default, Mole Fractions is already selected as Basis.
03:19 For Benzene enter 0.4 and press Enter.
03:24 For Toluene enter 0.6 and press Enter.
03:30 On the right, click on the Accept Changes button.
03:34 Now we will specify the Feed stream properties.
03:38 Go to Input Data.
03:40 Under Stream Conditions tab, select Flash Spec as Pressure and Vapor Fraction. (PVF)
03:48 Change Pressure to 1 atmosphere and press Enter.
03:53 Change Molar flow to 100 Kmol per hour and press Enter.
03:59 Now locate Vapor Phase Mole Fraction.
04:03 Here the default value is 0.
04:05 This indicates that the liquid is saturated.

Let us leave it as it is.

04:10 Now let us insert a Shortcut Column into the flowsheet.
04:15 At the bottom of the main simulation window, go to Columns tab.
04:20 The Shortcut Column is based on Fenske-Underwood-Gilliland method.
04:25 From the displayed list, drag and drop a Shortcut Column to the Flowsheet
04:30 Now let us insert two output streams.
04:34 To do that, let us drag one Material Stream.
04:38 Leave that stream as unspecified.
04:42 Then we will change the name of this stream to Distillate.
04:47 Next, we will insert another Material Stream.
04:51 Leave that stream as unspecified.
04:54 Let us change the name of this stream to Bottoms.

Press Enter.

05:00 Let us now insert two Energy streams for Condenser duty and Reboiler duty.
05:06 Go to Streams tab.

From the displayed list, drag and drop two Energy Streams to the Flowsheet.

05:14 Let us now arrange it as required.
05:17 Name these streams as C-Duty and R-Duty.
05:23 We are now ready to specify the Shortcut distillation column.

So let’s click on it.

05:29 On the left, we can see a tab displaying properties related to the Shortcut Column.
05:35 Under Connections, click on the drop-down against Feed Stream.

Select Feed.

05:43 Click on the drop-down against Distillate Stream and select Distillate.
05:50 Click on the drop-down against Bottoms Stream and select Bottoms.
05:57 Click on the drop-down against Condenser Duty and select C-Duty.
06:04 Click on the drop-down against Reboiler Duty and select R-Duty.
06:10 This completes the connectivity of the flowsheet.
06:13 Now, go to the Calculation Parameters.
06:17 This section is used to specify various attributes of a Shortcut Column.
06:22 Click on the drop-down against Light Key Compound (LK) and select Benzene.
06:31 Click on the drop-down against Heavy Key Compound (HK) and select Toluene.
06:39 Now go to Condenser Type.

By default, it is Total Condenser.

06:45 If a partial condenser is required, we can change it here.
06:49 Click on the field against LK Mole Fraction in Bottoms and enter it as 0.01 and press Enter.
06:58 Click on the field against HK Mole Fraction in Distillate and enter it as 0.01

Then press Enter.

07:08 Let us go back to the slides.
07:11 Recall that we want our reflux ratio to be 1.4 times the minimum reflux ratio.
07:18 So let us check the minimum reflux ratio.
07:22 For this, let us run simulation once.
07:26 To do this, click on Solve Flowsheet button.
07:30 Click on the Distillation Column.
07:33 From the Property Editor Window, locate Results section.
07:38 Now we can see that Minimum Reflux Ratio is 1.655.

So the actual Reflux Ratio will become 2.317.

07:49 Next let us enter the reflux ratio.
07:53 Look at the Shortcut Column results.
07:56 Here note the Actual Number of Stages and Optimal Feed Stage.

We can see that these values are NaN.

08:05 This is because the default value of reflux ratio is 1.5.

It is less than minimum reflux ratio.

08:14 Now let us enter the Reflux Ratio.
08:18 Enter the value as 1.655 into 1.4 and press Enter.
08:26 Now the Reflux Ratio is 2.317.
08:31 Click on the field against Condenser Pressure and enter it as 1 atmosphere

and press Enter.

08:40 Click on the field against Reboiler Pressure and enter it as 1 atmosphere .

Then press Enter.

08:48 Now we will run the simulation.
08:51 To do this, click on the Solve Flowsheet button on the toolbar.
08:56 When calculations are completed, click on the Shortcut column.
09:01 From the Property Editor Window, locate Results section.
09:06 This shows all the required results like:
09:09 Minimum Reflux Ratio
09:11 Minimum Number of Stages
09:14 Actual Number of Stages
09:17 Optimal Feed Stage
09:19 Condenser Duty, Reboiler Duty, etc
09:24 I have tabulated these results in a slide.
09:28 Let us go back to the simulation.
09:31 Let me save this.

I will save it as shortcut-end.

09:38 Let's summarize.
09:40 In this tutorial, we have learnt to:
09:42 Simulate a Shortcut distillation column, Calculate Minimum number of stages, Calculate Minimum reflux ratio, Calculate Optimal Feed stage location , Calculate Condenser and Reboiler duty
09:58 As an assignment,

Repeat this simulation with different compounds., Different feed conditions.

10:06 Different Column Properties.
10:08 This brings us to the end of this tutorial.
10:11 Watch the video available at the following link.

It summarizes the Spoken Tutorial project.

10:17 The Spoken Tutorial Project Team

Conducts workshops and Gives certificates.

10:22 For more details, please write to us.
10:25 Please post your time queries in this forum.
10:29 The FOSSEE team coordinates conversion of existing flowsheets into DWSIM.
10:35 We give honorarium and certificates for those who do this.

For more details, please visit this site.

10:44 The FOSSEE team helps migrate commercial simulator labs to DWSIM.

We give honorarium and certificates for those who do this. For more details, please visit this site

10:58 Spoken Tutorial and FOSSEE projects are funded by NMEICT, MHRD, Government of India.
11:07 We thank the DWSIM team for making it as an open source software.

This tutorial was originally recorded by Prof Kannan Moudgalya in May 2015.

11:19 This is Kaushik Datta from IIT Bombay. Thanks for joining.

Contributors and Content Editors

PoojaMoolya